Possible apparatus:Simple DistillationFractional DistillationSteam DistillationExtraction (Separatory funnel)Simple Reflux RefluxApparatuswith Addition Assembly*Techniques (microscale and miniscale)–All of the techniqueslearned this semester are summarized below. Be ready to discuss them with the TA giving the exam or answer written questions pertaining to these techniques. Questions will be general and test yourknowledge of theory of the techniques and manipulations.If you have paid attention and learned during the semester, little studying should be required. Filtrations (gravity versus vacuum)Recrystallization (four steps)RefluxSublimationDrying agentsExtraction Thin-Layer ChromatographyColumn ChromatographySimple distillationFractional distillationGas ChromatographyDesiccatorsMelting PointsBoiling PointsSteam DistillationMicrofiltrationsReagent additions during reactionNMR and IR sample preparationsCalculationsKnow how to determine the limiting reagent and calculate all types of yields using data given such as masses, moles, densities, balanced equations, etc. Also, be able to calculate the quantity of a reagent required to obtain such and such yield from a reaction. Other-Answer questions related to waste handling, safety, notebook documentation, and laboratory protocols.
